本書是為適應信息化和國際化教育需求而編寫的。全書共5章,包括緒論、基本操作和常用儀器、基礎無機化學實驗、基礎分析化學實驗、綜合設計實驗。每個實驗配有詳盡的背景知識、實驗原理、實驗步驟、安全提示和廢棄物處理等;絕大部分實驗有拓展部分,以滿足教學高階性的需求。本書雙語模式獨具特色,以滿足不同英文水平學習者的需求。本書還配套了62個最新完成的高質量視頻,讀者掃描書中二維碼即可觀看學習。
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1992.9-1995.7,原杭州大學化學系碩士研究生學習,獲得理學碩士學位;
1998.3-2003.3,浙江大學環(huán)境與資源學院博士生學習,獲得工學博士學位;
1995-1998,原杭州大學化學系,講師
1998-2017,浙江大學化學系,講師、副教授
2017--至今,浙江大學化學系,正高級實驗師
目錄
Preface
前言
Chapter 1 Introduction 緒論 1
1.1 Chemistry Laboratory Safety Policies 化學實驗室安全制度 1
1.2 Requirements for the Course 課程要求 6
1.3 Guidelines for Lab Notebook, Pre-lab, and Post-lab Report 實驗記錄本、預習報告和實驗報告指南 9
1.4 Introduction to Titrimetric Analysis 滴定分析法概述 12
1.5 Significant Figures and Data Treatment 有效數(shù)字和數(shù)據(jù)處理 16
Chapter 2 Basic Operations and Common Instruments 基本操作和常用儀器 22
2.1 Cleaning and Drying Glassware 玻璃器皿的洗滌和干燥 22
2.2 Transferring Reagents 試劑的取用 24
2.3 Use of Volumetric Glassware 量器類玻璃器皿的使用 25
2.4 Separation Techniques 分離技術 32
2.5 Common Instruments 常用儀器 36
Chapter 3 Fundamental Inorganic Chemistry Experiments 基礎無機化學實驗 47
Expt. 1 Separation and Identification of Common Cations 常見陽離子的分離和鑒定 47
Expt. 2 Separation and Identification of Common Anions 常見陰離子的分離和鑒定 53
Expt. 3 Determination of Reaction Rate Constant, Activation Energy and Influencing Factors 反應速率常數(shù)、活化能及影響因素的測定 60
Expt. 4 Preparation of Alum and Large Crystal Cultivation 明礬的制備及其大晶體培養(yǎng) 66
Chapter 4 Fundamental Analytical Chemistry Experiments 基礎分析化學實驗 72
Expt. 5 Preparation and Standardization of the Solutions for Acid-base Titration 酸堿滴定溶液的配制與標定 72
Expt. 6 Preparation and Standardization of the Solutions for Redox Titration 氧化還原滴定溶液的配制與標定 77
Expt. 7 Preparation and Standardization of the Solution for Complexometric Titration 配位滴定溶液的配制與標定 84
Expt. 8 Preparation and Standardization of the Solution for Precipitation Titration 沉淀滴定溶液的配制與標定 88
Expt. 9 Practise of Basic Operations for Titrimetric Analysis 滴定分析基本操作訓練 92
Expt. 10 Determination of the Molecular Weight of an Unknown Diprotic Organic Acid 未知二元有機酸分子量的測定 95
Chapter 5 Comprehensive and Designing Experiments 綜合設計實驗 98
Expt. 11 Determination of the Fluoride Content in Tea Samples by FISE 氟離子選擇電極法測定茶葉中氟離子含量 98
Expt. 12 Preparation and Characterization of Mohr’s Salt 莫爾鹽的制備及表征 104
Expt. 13 Preparation and Characterization of Copper Methionine 蛋氨酸銅的制備及表征 107
Expt. 14 Preparation and Photosensitivity Test of Potassium Trioxalatoferrate(III) Trihydrate 三水合三草酸合鐵(III)酸鉀的制備及光敏性測試 111
Expt. 15 Determination of the Charge Number of Trioxalatoferrate(III) Complex Ion 三草酸合鐵(III)配離子電荷數(shù)的測定 115
Expt. 16 Spectrophotometric Determination of Iron Content 分光光度法測定鐵含量 118
Expt. 17 Synthesis and Characterization of Three Kinds of Cobalt-ammine Coordination Compounds 三種鈷氨配合物的制備及表征 126
Expt. 18 Determination of Cement Composition 水泥組分測定 132
Expt. 19 Preparation and Determination of Three Kinds of Sodium Phosphate Hydrates 三種磷酸鈉鹽水合物的制備及測定 139
Expt. 20 Preparation of Heteropolyacid Salts and Determination of Conversion Kinetics 雜多酸鹽的制備及其轉化動力學測定 144
APPENDIX 151
Appx. 1 Illustration of Common Glassware and Apparatus 常用玻璃器皿和儀器插圖 151
Appx. 2 Vocabulary of Common Professional Words and Phrases 常用專業(yè)詞匯中英文對照表 152
Appx. 3 Density, Content and Concentration of Common Concentrated Acids and Bases 常用濃酸、濃堿的密度、含量和濃度 157
Appx. 4 Common Indicators 常用指示劑 157
Appx. 5 Color of Common Ions and Inorganic Compounds 常見離子和無機化合物的顏色 159
Appx. 6 Bilingual Videos Embedded in the Manual 本書插入雙語視頻清單 160
Appx. 7 Atomic Weight of Elements 元素的原子量 162